FED-STD-791D
1.4 Crystallizing dish, 9 cm diameter H 5.0 cm deep
1.5 Graduated cylinders, 50 and 100 mL
1.6 Separatory funnel , pear shaped ,250 mL
1.7 Erlenmeyer flask, narrow mouth, glass stoppered, 300mL
1.8 Erlenmeyer flask narrow mouth , standard taper joint, 300mL
1.9 Vigreux fractionating column, standard taper joint at lower end
complementary to joint of flask described in 4.11
1.10 Syringe, 10-L capacity, graduated in 0.2L.
1.11 Analytical balance, 200 g capacity
1.12 Vacuum oven
1.13 Vacuum pump
1.14 Electric stirrer
1.15 Electric vibrator
1.16 Filter , size 4.7 cm diameter, 10 L.
1.17 Stainless filter holder and funnel
5. MATERIALS
5.1 CAUTION: SOME MATERIALS ARE TOXIC AND HAZARDOUS . The
materials and standards listed in this section must be handled carefully. Federal test
method 10000 , Material Handling Safety Precautions, is a reference which lists all toxic
and hazardous material cited in FTMS 791. The synonyms, life hazard, flammability,
handling and storage precautions, emergency treatment and measures and spill practices
of each chemical are explained.
5.2 Potassium hydroxide, reagent grade [3,0,1].
5.3 Ethyl alcohol, 95% [0,3,0].
5.4 Distilled water
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