FED-STD-791D
handling and storage precautions, emergency treatment and measures, and spill practices
of each chemical are explained.
5.2 Test sheets (3), rubber standard, type as required by the specification,
approximately 2.5 H5.1 H 0.19 cm. Samples of synthetic rubber stock should not be
older than 6 mo.
5.3 Alcohol, ethyl or methyl, anhydrous [1,3,0].
5.4 Filter paper.
5.5 Distilled water.
6. PROCEDURE
6.1 Determine the water displacement of each test sheet to the nearest 1 mg by
weighing each sheet in air, then in distilled water at 24 " 3C, recording the weights,
and computing the difference between the weight in air and the weight in water for each
sheet (see 7.1).
6.2 Fill container with sample, using the following:
a. For liquid sample: Approximately 20 mL of sample for each gram of total
weight of test sheets.
b. For grease sample: Sufficient sample to fill container completely.
6.3 Blot dry each test sheet with filter paper, then immerse sheets completely in
sample in container. For grease samples, immerse test sheets vertically, with 5 cm edge
uppermost, and cover the container.
6.4 Store container in oven at 70 " 1C (158 " 2F) for 168 " 0.5 h
(approximately one week). For liquid samples, maintain a ratio of 20 mL of oil to each
gram of test sheet. Make up oil must be the same temperature as the test fluid when
added. For grease samples, check daily (except weekends), that the samples are in
complete contact with test sheets and close any voids by using a spatula.
6.5 At the end of the storage period, cool the sample to 24 " 3C. Then clean
test sheets as follows:
a. Remove test sheets from sample and wipe them to remove most of the adhering
sample.
b. Dip sheets in alcohol and wipe or blot them dry, using filter paper (or soft
cloths). NOTE THE TIME.
6.6 Within 5 min of drying test sheets, redetermine the water displacement of
each sheet as specified in 6.1.
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